摘要
利用1HNMR、13CNMR、DEPT等一维谱和1H-1HCOSY、HSQC、HMBC及1H-1HNOESY等二维核磁共振波谱技术确定了6种内型-8-烷氧基甲基异莰烷类化合物的结构,并对其1H、13CNMR信号进行了全归属,初步探讨了取代基对化学位移的影响.此6种化合物的核磁数据可作为该类化合物的参考.
The structures of 6 endo-8-alkoxylmethylisocamphane derivatives were determined by 1 D-NMR spectroscopy(~1 H NMR、^(13) C NMR、DEPT) and 2 D-NMR spectroscopy (~1 H—~1 H COSY、HSQC、HMBC、~1 H—~1 H NOESY). All the ~1 H and ^(13)C NMR data were assigned, and the varieties of chemical shifts with the substitute of the compounds were discussed. The NMR data of these compounds can be used as the reference of these series compounds.
出处
《江西师范大学学报（自然科学版）》
CAS
2004年第2期129-131,共3页
Journal of Jiangxi Normal University(Natural Science Edition)
基金
江西师范大学青年成长基金资助项目
江西省自然科学基金(972036)资助项目.
