摘要
分析了化学镀工艺对Ni—Fe—P镀覆织物镀速的影响，确定了涤纶织物铁镍化学镀工艺；测试了铁镍复合涤纶织物的电阻，并利用扫描电子显微镜（SEM）对镀层的表面形态进行表征。结果表明，较好的铁镍化学镀工艺为：盐总摩尔浓度（CNi/CFe2＋=9：1）为0．1mol／L，硼酸0.3mol／L，硫脲0．03mmol／L，pH值10．0-10．5，施镀温度90℃，施镀时间1h；最大镀速达到3．289g／（min·m2），镀层的表面电阻值为5．08Ω／sq。扫描电镜显示，铁镍镀层均匀连续，铁镍合金微粒的大小约为0．5μm。
The effect of chemical plating process on plating speed of Ni-Fe-P onto fabric are analyzed,and the appropriate process for plating Ni-Fe onto PET fabrics is established. The resistance of iron-nick-el composited PET fabrics are measured, and microstructure of coating surface morphology is observedwith Scanning Electron Microscopy （SEM）. The results show that the optimal parameters of chemicalplating process is： total salt （CNi/CFe2＋=9：1）0.1 mol/L, boric acid 0.3 mol/L, thiourea 0.03 mmol/L, pHvalue 10.0-10.5, plating at 90 ℃ for 1 h; the maximum deposition rate can reach 3.289 g/（min, m2）, andthe electric resistance of coating surface can reach 5.08 Ω/sq. Scanning electron microscopy shows thata uniform and continuous iron nickel coating can be formed with the size of iron nickel alloy particles ofabout 0.5 μm.
出处
《印染》
北大核心
2015年第5期15-18,共4页
China Dyeing and Finishing
基金
南通大学杏林学院科研项目(项目编号2014K123)
江苏省科技厅产学研协同创新前瞻项目(项目编号BY2012131)
关键词
功能性整理
化学镀
铁
镍
涤纶织物
functional finish
chemical plating
iron
nickel
polyester fabric
