摘要
目的确定当仁通便灵颗粒的最佳乙醇提取工艺。方法以阿魏酸的含量为指标,采用正交试验(L934)优选提取工艺条件。结果影响醇提工艺的因素的程度依次为提取次数、乙醇体积分数、提取时间和固液比。最适工艺条件为加6倍量70%乙醇,加热回流提取2次,每次1.5h。结论工艺稳定、可行。
Objective To optimize the extraction procedure of Dangren Tongbianling Particles . Methods The extraction ratio Of the content of Ferulic Acid was used as index, and the optimum condition of the extraction was studied by the orthogonal L9 ( 34 ). Results The influencing effects of factors were as follow C 〉 A 〉 D 〉 B(A:alcohol concentration,B:liquid - solid ratio ,C:extraction times,D:extraetion time). The optimize extraction condition was as follows : adding 6 times of 70% alcohol , refluxing for 2 times, 1.5 hours every time. Conclu- sion The optimum extraction procedure is stable and practical.
出处
《湖北中医药大学学报》
2014年第1期49-51,共3页
Journal of Hubei University of Chinese Medicine
关键词
当仁通便灵颗粒
正交试验
阿魏酸
Dangren Tongbianling Particles
orthogonal test
ferulic acid