摘要
目的 :建立八宝眼粉的质量控制方法。方法 :采用化学反应和薄层色谱法 (TLC)鉴别方中炉甘石、人工牛黄、冰片 ;采用气相色谱法 (GC)测定冰片的含量。结果 :鉴别效果满意 ;冰片在 0 .0 980 8～ 0 .784 6 4 μg范围内呈良好的线性关系 ,平均加样回收率为 1 0 1 .5 %,RSD =1 .4 0 %(n =5 )。结论 :本方法简便、快速准确 ,可作为该制剂质量控制方法。
OBJECTIVE To establish a quality standard for Babao Eye Powder. METHODS Galamina?Artificial calculus bovis and synthetic borneol were indentity by chemical reaction and TLC; synthetic Borneol was determined by GC. RESULTS The average recovery was 101.5% ,RSD= 1.40% ( n =5).CONCLUSIONS The methods are suitable for the quality control of the powder.
出处
《中国医院药学杂志》
CAS
CSCD
北大核心
2004年第4期210-211,共2页
Chinese Journal of Hospital Pharmacy
