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低温陈化法制备ε-Zn(OH)_2晶体及其表征 被引量:1

Preparation and characterizatinon of ε-Zn(OH)_2 crystals by aging at low temperature
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摘要 ε-Zn(OH)2 crystals with high thermal stability,well crystallinity and fine dispersity were prepared by aging at low temperatue from zinc nitrate and sodium hydroxide in aqueous solution. The crystal structure,morphology and thermal stability were characterized by Xray diffractometry,scanning electron microscopy and differential scanning calorimeter. The influences of reaction temperatures,mole ratios of zinc nitrate to sodium hydroxide and phase-inversion rates on the products were discussed in details. ε-Zn(OH)_2 crystals with high thermal stability,well crystallinity and fine dispersity were prepared by aging at low temperatue from zinc nitrate and sodium hydroxide in aqueous solution. The crystal structure,morphology and thermal stability were characterized by Xray diffractometry,scanning electron microscopy and differential scanning calorimeter. The influences of reaction temperatures,mole ratios of zinc nitrate to sodium hydroxide and phase-inversion rates on the products were discussed in details.
出处 《化学研究与应用》 CAS CSCD 北大核心 2004年第1期99-100,共2页 Chemical Research and Application
基金 河北省自然科学基金资助课题(501115)
关键词 氢氧化锌晶体 ε—Zn(OH)2晶体 制备 低温陈化 表征 斜方晶体 液相合成 ε-Zn(OH)_2 crystal preparation aging at low temperature
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