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从乌贼内壳提取β-壳聚糖及其结构表征 被引量:7

Isolation and Structural Characterization of β- chintosan of Sepia Shell
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摘要 研究了用乌贼内壳制备β-甲壳素和壳聚糖,结果乌贼内壳背木盾提取甲壳素的最佳条件为:先用1.5mol/LHCl浸24h,再用1.5mol/L NaOH于80℃浸3h,产率为3.55%。从乌贼内壳周缘提取甲壳素的最佳条件为:先用1.5mol/L HCl浸24h,再用1mol/L NaOH 75℃浸3h,产率为30.00%;产品用IR和XRD表征。致突变试验结果表明用乌贼内壳制备的β-壳聚糖无致突变性。 Isolation of β- chintin and chintosan from sepia shell had been studied and the best condition of extracting chintinfrom sepia shell (hard bone) was: soaked with 1.5mol/L HCl for 24h first, then soaked with 1.5mol/L NaOH at 80℃ for another3h. The extraction ratio was 3.55%. The best condition of extracting chintin from its soft bone was: soaded with 1.5mol/L HClfor 24h first, then soaked with 1mol/L NaOH at 75℃ for another 3h. The extraction ratio was 30.00%. Final product wascharactered by IR and XRD. The result also showed that β- chintosan was safety.
出处 《食品科学》 EI CAS CSCD 北大核心 2004年第1期105-107,共3页 Food Science
关键词 β—壳聚糖 壳聚糖 结构表征 乌贼内壳 提取 chintin chintosan sepia
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