摘要
以芴为原料 ,经甲醛羟甲基化反应合成了新型给电子体 1,3-双醚的前体 ,总收率达 6 5 % ,并对生产工艺进行了优化研究。
Used sodium ethoxide/alcohol solution as catalyst and 1,3-disther as material, 9,9-bis(hydromethyl) fluorene was synthesized through method of hydromethylation. The influence factors of yield were discussed. The optimum reaction processes were studied.
出处
《化工技术与开发》
CAS
2003年第5期4-5,26,共3页
Technology & Development of Chemical Industry
