摘要
考察了RuO_4相转移催化氧化法合成对硝基苯甲酸的各种影响因素。讨论了次氯酸钠纯度对氧化反应的影响。在优化条件下对硝基苯甲酸的收率为87.3％,产品纯度为99％。
Various factors affecting the preparation of p-nitrobenzoic acid by PTC-RuO_4-NaClO method were investigated. The influence of NaClO purity to the oxidation reaction was discussed. The yield of p-nitrobenzoic acid under optimized conditions is 87.3%. The purity of the product is 99%.
出处
《精细石油化工》
CAS
CSCD
1992年第3期31-35,共5页
Speciality Petrochemicals
关键词
对硝基苯
甲酸
相转移催化
氧化
p-nitrobenzoic acid
Ruthenium Tetraoxide
Sodium Hypochlorite
Phase Transfer Catalysis
Oxidation
