摘要
目的建立蒲黄用柠檬黄非法染色的检查方法。方法采用TLC法、HPLC-PAD法,对多批次蒲黄样品进行定性定量分析。结果经检测10批市售样品中,有6批检出柠檬黄,其含量在0.05~0.50mg/g。结论蒲黄染色除用化工原料金胺O外,还有用柠檬黄染色现象,本文所建立的检测方法,可以满足蒲黄用柠檬黄染色定性定量的要求。
Objective Establish inspection methods Typhae Pollen illegal stained with tartrazine. Methods The technique of TLC and HPLC-PAD were developed for qualitation and quantitative analysis mutiple batches of samples Typhae Pollen.Results After testing 10 batches of commercial samples, six batches detected in lemon yellow, its content in the 0.05-0.50mg/g. Conclusion The use of chemical raw materials except Typhae Pollen staining outside auramine, there are lemon yellow staining phenomenon, The method established in this paper, to meet with tartrazine stain Typhae Pollen qualitative and quantitative requirements.
出处
《中国医药科学》
2015年第19期69-71,74,共4页
China Medicine And Pharmacy
