摘要
室温下用氢氧化钾将邻苯二甲酰亚胺转化为钾盐 ,然后使其与 1 ,4 -二溴丁烷在丙酮中回流反应 ,制得 N-( 4-溴丁基 )邻苯二甲酰亚胺 ,产率达 90 %
Phthalimide was treated with potassium hydroxide in ethanol at room temperature to give potassium phthalimide,which was refluxed with 1,4 dibromobutane in acetone to give N (4 bromobutyl)phthalimide in high yield (up to 90%).
出处
《化学试剂》
CAS
CSCD
北大核心
2001年第6期359-359,361,共2页
Chemical Reagents