摘要
Hexachlorocyclotriphosphazene was prepared by reacting ammonium chloride and phosphorus pentachloride in an inert organic solvent at the presence of different metal compounds and pyridine. The conbination of MgCl2·6H2O with pyridine showed an ideal catalytic activity to give hexachlorocyclotriphosphazene in yield of 87% under the suitable conditions. The method is time saving.
Hexachlorocyclotriphosphazene was prepared by reacting ammonium chloride and phosphorus pentachloride in an inert organic solvent at the presence of different metal compounds and pyridine. The conbination of MgCl_2·6H_2O with pyridine showed an ideal catalytic activity to give hexachlorocyclotriphosphazene in yield of 87% under the suitable conditions. The method is time saving.
出处
《应用化学》
CAS
CSCD
北大核心
2001年第2期163-164,共2页
Chinese Journal of Applied Chemistry
基金
航空院校自选课题基金
关键词
三聚磷腈
氯化铵
五氯化磷
催化合成
hexachlorocyclotriphosphazene,ammonium chloride,phosphorus pentachloride,synthesis