摘要
采用甲基二氯氢硅（ＣＨ３ＨＳｉＣｌ２）与环己烯（Ｃ６Ｈ１０）为原料，在铂催化剂作用下，经加成反应，合成目标产物，并对精馏等工艺条件作了初步实验。获得高纯度（≥９９％）的 ＣＨ３Ｃ６Ｈ１１Ｓｓｉ（ＯＣＨ３）２。
In this paper,the synthetic method has been discussed by addition reaction between cyclohex ene( C5 H10) and methyl dichlorosilane ( CH3HSiC12) with platinic catalyst and the conditiens of rectification for reaction mixture have been studied. The reaction mixture can produce the desired methyl cyclohexyl dimethoxyl silane(CH3C6H11Si(OCH3)2) with a purity of above 99 %.
出处
《上海工程技术大学学报》
CAS
1999年第2期122-127,共6页
Journal of Shanghai University of Engineering Science
关键词
二甲氧基硅烷
加成反应
有机硅化合物
硅氧烷
Metyl cyclohexyl dimethoxy silane Addition reactions Cyclohexene Gas chromatographic analysis Rectification
