期刊文献+

甲胺磷原油中硫酸二甲酯的正相高效液相色谱分析 被引量:5

Analysis of Dimethyl Sulfate in Methamidophos Technical by Postived-Phase High Performance Liquid Chromatgraphy
在线阅读 下载PDF
导出
摘要 采用 C18 柱,示差折光检测器,以7030( 体积比) 正己烷 异丙醇为流动相的正相高效液相色谱对甲胺磷原油中的硫酸二甲酯进行了分析,方法准确,快速,其平均回收率为98 .4 % ,相对标准偏差小于0 .5 % . Dimethy sulfafe in methamidophos technical has been analyzed by postive phase highperformnace Liquid chromaography with C 18 column,RID-6A dectector,and n-Hexane/Isopropanal (V/V) 70/30 as mobile phase The method is acurate and rapid,its average recovery rate is 98.4%,and the relative standard deviaton is less than 0.5%.
出处 《湘潭大学自然科学学报》 CAS CSCD 1999年第3期41-41,共1页 Natural Science Journal of Xiangtan University
基金 湖南省教委重点资助项目
关键词 甲胺磷原油 硫酸二甲酯 高效液相色谱 methamidophos thchnical,dimethyl sulfate,positive-phase high perfomamce liquid chromatography
  • 相关文献

同被引文献34

  • 1覃宣富,邹晓莉,黎源倩,曾红燕,李岩.气相色谱-电子捕获检测测定环境样品中的硫酸二甲酯含量[J].四川大学学报(医学版),2010,41(5):877-880. 被引量:15
  • 2胡九成,刘之定.催化裂化反应动力学参数识别与优化[J].化学反应工程与工艺,1994,10(2):124-131. 被引量:3
  • 3Atukazu I. Method for Purifying O,S-Dimethyi N-Acetyiphosphoramidothioate. Mexico, MXPA 99007019. 2004
  • 4罗和安,王良芥,刘平乐等.高纯度乙酰甲胺磷原粉的制备方法.中国,CN02113934.2004
  • 5Prasad V A, Jeiich K, Smith D K. An Improved Process for Making O,S-Dimethyi phosphoramidothioate. Canada, CA 225416. 1999
  • 6李坚.高含量甲胺磷的制备方法.中国,CN1727352A.2006
  • 7Charpentier J C, Mckenna T F. Managing Complex Systems: Some Trends for the Future of Chemical and Process Engineering. Chemical Engineering Science, 2004, 59 (8-9): 1617-1640
  • 8Ferrouillat S, Tochon P, Della D V, et al. Open Loop Thermal Control of Exothermal Chemical Reactions in Multifunctional Heat Exchangers. International Journal of Heat and Mass Transfer, 2006, 49 (15-16): 2479-2490
  • 9Li H, Wang SW,Zhang BL, et al mination of 9 active components Simuhaneous quantitative deter- in traditional Chinese medicinal preparation ShuangDan oral liquid by RP-HPLC coupled with pho- todiode array detection[ J]. Journal of Pharmaceutical and Biomed- ical Analysis ,2011,56(4 ) :820 - 824.
  • 10薛芬,戴华娟,王建中,等.丹皮酚(2-羟基-4-甲氧基苯乙酮)的合成[J].上海第一医学院学报,1984,11(4):312-313.

引证文献5

二级引证文献26

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部