摘要
用微波法制备纳米水合二氧化锆,通过包覆工艺,将Y(OH)_3均匀地包覆在水合二氧化锆粒子表面,制备出ZO_2(3Y)的先驱体.然后用聚甲基丙烯酸铵(PMAA-NH_4)对α-Al2O3、纳米SiC及包覆水合二氧化锆表面改性.使三种单相水悬浮液在PH=9.0时,粒子表面电性相同,且有良好分散状态.从而制备出高分散、均混合Al2O3-SiC-ZrO2(3Y)先驱体水悬浮液.
Zro2(3Y) precursor was prepared via hydrous-zirconia which was Y(OH)3-coated preparedby microwave heating coated with Y(OH)3. The surfaCes of Al2O3, nanometer SiC and Y(OH)3coated hydrous-zirconia particles were modified with PMAA-NH4, so that three kinds of periclesin aqueous suspensions had the same charge and highly dispersed state at PH=9.0. Finally, ahighly dispersed and uniformly mixed suspension of Al2O3-SiC-ZrO2(3Y) precursor was obtainedfrom miting three kinds of single suspension.
出处
《无机材料学报》
SCIE
EI
CAS
CSCD
北大核心
1999年第1期43-48,共6页
Journal of Inorganic Materials
基金
国家自然科学基金!59572010
清华大学新型陶瓷与精细工艺国家重点实验室资助
关键词
胶体
改性
分散
混合
悬浮液
复合陶瓷
colloidal behaviour, surfaCe modification, highly dispersed suspension, uniformlymixed suspension