摘要
以活性炭负载硫酸作为一种新型、便宜且有效的环境友好固体催化剂,催化合成了橙花素.考察了反应时间、无水乙醇用量、催化剂用量对合成工艺的影响,确定了最佳反应条件为n(β-萘酚)∶n(无水乙醇)=1∶8,催化剂用量1.2 g,反应时间5 h,反应温度80℃.在此条件下,橙花素产率为91.8%.
Nerolin bromelia was synthesized in the presence of a new environmentally friendly catalyst H2SO4/carbon.The influences of catalyst＇s dosage,ethanol consumption,and the reaction time on the yield of product have been investigated.Get the optimal reaction conditions as follows： n（β-naphthol）∶n（ethanol）=1∶8,amount of catalyst is 1.2 g,reaction time is 5 h and the temperature is 80 ℃.Under the optimal reaction condition,a 91.8% yield of nerolin bromelia were obtained.
出处
《宁夏大学学报（自然科学版）》
CAS
北大核心
2010年第2期162-164,共3页
Journal of Ningxia University(Natural Science Edition)
基金
国家自然科学基金资助项目(20562010)
国家"973"基金资助项目前期预研专项(2006CB708606)
教育部科学技术研究重点基金资助项目(203143)
宁夏自然科学基金资助项目(NZ0816)
关键词
橙花素
改性活性炭
催化
合成
nerolin bromelia
modified activated carbon
catalyst
synthesis
