摘要
采用固相萃取净化技术及高效液相色谱法,测定西洋参冲剂中人参皂甙Rb1的含量.结果在12.5~200μg/ml范围内,Rb1的含量与峰面积呈良好线性,平均回收率及RSD分别为:101.33.2%(0.4mg,n=5):101.22.6%(0.2mg,n=5);99.04.4%(0.1mg,n=5).最小检出量为0.3μg,本法简便、快速、准确。
Ginsenoside Rb1 in panax quinquefolius linn granules was deterrnined by solidphase extraction technique and by HPLC. Its range was 12. 5~200μg. ml,Rb_1 expressed a goodlinearity(r= 0. 99996). The mean recovery and RSD of Rb1 were 101. 3 3. 2 % (0. 4mg,n= 5) ;101. 2 2. 6 % (0. 2mg,n = 5); 99. 0 4. 4(0. 1mg , n = 5 )respectively. This method is simple andrapid.
出处
《天津药学》
1998年第1期79-81,共3页
Tianjin Pharmacy