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液相色谱-荧光法测定甲氨基阿维菌素苯甲酸盐在甘蓝和土壤中的残留 被引量:24

Determination of the Residual of Emamectin Benzoate in Cabbage and Soil with HPLC Fluorescence Detection
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摘要 利用反相高效液相色谱-荧光法分析测定土壤、甘蓝中甲氨基阿维菌素苯甲酸盐的残留量。甲氨基阿维菌素苯甲酸盐在10~500ng/ml(r=0.9996)范围内峰面积与进样量呈良好的线性关系,平均回收率甘蓝为95.61%,变异系数为0.4%;土壤中为81.4%,变异系数为4.9%。该法操作简便、快速,回收率较高。 The high performance liquid chromatographic method with fluorescence detection was used for the determination of emamectin benzoate in cabbage and soil. Good linearity of emamectin benzoate was obtained over the ranges of 10 - 500 ng/ml ( r = 0.999 6). The average recovery rate of emamectin benzoate was 95.61%( RSD 0.4%) in cabbage and 81.4%(RSD 4.9%) in soil .This method was simple,quick and the recovery rate was better.
出处 《安徽农业科学》 CAS 北大核心 2008年第18期7533-7534,共2页 Journal of Anhui Agricultural Sciences
关键词 高效液相色谱 甲氨基阿维菌素苯甲酸盐 残留检测 High performance liquid chromatography Emamectin benzoate Residue determination
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参考文献4

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  • 3王小丽,王素利,陈振山,刘丰茂.黄瓜及其栽培土壤中甲氨基阿维菌素苯甲酸盐的残留动态研究[J].农业环境科学学报,2005,24(z1):307-310. 被引量:19
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