摘要
以原位合成法制备的分子筛膜对玻璃毛细管内壁进行改性后,成功地制备了常现口径及大口径分配型SCOT柱,并对毛细管柱的性能进行了评价.
Various stationary phases with different polarity have been coated evenly on thesurface of in Situ synthesized zeolite membrane. The zeolite membrane modified gas columnhas been prepared. Some characteristics of this new kind of column such as columnefficiency, separating power, quantitative accuracy and thermostability of stationary phasehave been evaluated. Large-bore zeolite membrane SCOT column has also been parpared inorder to replace the packed column in regular analysis. its column capacity and separationpower under the condition of split stream and no supplemental gas have been studied.
出处
《高等学校化学学报》
SCIE
EI
CAS
CSCD
北大核心
1997年第9期1442-1446,共5页
Chemical Journal of Chinese Universities
基金
国家自然科学基金
天津市自然科学基金
关键词
气相色谱
原位合成
分子筛膜
毛细管柱
SCOT柱
Gas chromatography, In situ synthesis, Zeolite membrane, SCOT capillary column