摘要
目的：制备益肝康口服液并建立其质量标准。方法：采用薄层色谱（TLC）法对方中黄芪、党参、丹参进行定性鉴剐；采用高效液相色谱（HPLC）法对党参炔苷进行含量测定。结果：TLC中特征斑点明显；党参炔苷检测浓度在0．036-1．317mg·mL^-1范围内与峰面积积分值呈良好线性关系（r=0．9999）；平均加样回收率为100．10％，RSD=1．70％（n=6）。结论：制备方法简便、可靠；所建标准可用于益肝康口服液的质量控制。
OBJECTIVE： To prepare Yigankang oral liquid and establish its quality criteria.METHODS： The constituents such as Radix Astragali, Radix Codonopsis and Radix Salvia Miltiorrhiza in Yigankang oral liquid were identified by TLC. The content of Lobetyolin in Yigankang oral liquid was determined by HPLC. RESULTS： The characteristic TLC spots were noted. Lobetyolin showed a good linear relationship in the a range of 0.036-1.317 mg . mL ^-1（r = 0.999 9） and the average recovery was 100.10% with RSD at 1.70%. CONCLUSION： The method is simple and reliable, and it can be used for the quality control of Yigankang oral liquid.
出处
《中国药房》
CAS
CSCD
北大核心
2008年第3期192-194,共3页
China Pharmacy
