摘要
建立了电感耦合等离子体发射光谱法测定水中铀的方法。优化了仪器工作条件，通过基体匹配消除了无机酸基体干扰。方法检出限为0．15mg／L，对5．0000mg／L铀标准溶液测定的相对标准偏差（RSD）为0．98％（n=10），加标回收率为95％～106％，方法准确可靠。
A method for the determination of uranium in water by inductively coupled plasma atomic emission spectrometry（ ICP- AES） was developed. Instrumental operating parameters were optimized, and the matrix effect of inorganic acid was eliminated through matrix matching. The detection limit was 0. 15 mg/L and the RSD was 0. 98% for 5.000 0 mg/L uranium solution （ n = 10 ）. The recovery- range was 95%-106%. The accuracy of the method was verified by analyzing the Standard（GBW（E）080173） under optimized operating conditions. The result obtained agreed quite well with that of the Standard.
出处
《分析测试学报》
CAS
CSCD
北大核心
2007年第6期845-846,850,共3页
Journal of Instrumental Analysis
