摘要
以环己酮和查尔酮为原料,在NaOH存在下无溶剂室温研磨反应,非常方便地得到Michael加成产物.该方法具有反应条件温和、操作简单和产率较高等优点,并通过IR,1H NMR和元素分析确证产物的结构.
A series of Michael addition products of cyclohexanone to chalcone were obtained in the presence of sodium hydroxide under solvent-free condition. The advantages of this procedure were mild reaction conditions, simple protocol, and high yields. The structures of the products were characterized by IR, ^1H NMR spectra and elemental analysis.
出处
《有机化学》
SCIE
CAS
CSCD
北大核心
2007年第10期1292-1295,共4页
Chinese Journal of Organic Chemistry
基金
徐州师范大学自然科学基金(No.06XLA09)资助项目