摘要
建立了有机化工产品中四丁基溴化铵残留测定的新方法。该法线性范围为0.01~0.10g/L,检出限为0.4mg/L,相对标准偏差为2.4%(0.05g/L,n=11),相关系数为0.998,用于实际样品测定,结果令人满意。
A new method for the determination of tetra-butyl ammonium bromide (TBAB) residua in organic chemical products by bromide ion-selective electrode was developed. The linear range of the calibration curve for TBAB was 0. 01 -0. 10 g/L with a correlation coefficient of 0. 998 5. The relative standard deviation was 2.4% (0. 05 g/L, n = 11 ) and the detection limit was 0.4 mg/L. The method has been used to determine TBAB residua in organic chemical products with satisfactory results.
出处
《分析测试学报》
CAS
CSCD
北大核心
2007年第3期428-430,共3页
Journal of Instrumental Analysis
关键词
溴离子选择电极
四丁基溴化铵
有机化工产品
Bromide ion selective electrode
Tetra-butyl ammonium bromide
Organic chemical products