摘要
采用微波消解样品、火焰原子吸收分光光度法（FAAS）测定了3种野菜中的钾、钠、钙、铜、镁、铁等无机元素的含量．考察了微波消解条件对分析结果的影响，同时选FAAS测定的最佳条件．利用该法对野菜中的9种无机元素进行了分析，方法回收率在96％～104％之间，相对标准偏差为1．02％～3．30％，测定结果令人满意．
The use of microwave digestion in the determination of K, Na, Ca, Cd, Cu, Mn, Pb, Mg, Fe in potherbs by FAAS was described. The optical condition of microwave digestion and FAAS measurement were also investigated. Compared with traditional wet digestion method, microwave digestion could be done more rapidly and effectively and displayed a lower background. Applied to the determination trace elements in potherbs the method proved to be selective with satisfactory recovery of 96 % - 104 % and relative standard deviation of 1.02 %-3.30 %.
出处
《河北师范大学学报（自然科学版）》
CAS
北大核心
2007年第1期90-92,共3页
Journal of Hebei Normal University：Natural Science
基金
河北省科学技术厅科技攻关项目(04220143)
河北师范大学青年基金(L2003Q16)
关键词
微波消解
测定
微量元素
FAAS
microwave digestion
determination
trace elements
FAAS
