摘要
采用了离子交换分离富集矿样中的锰,该系统与原子吸收测量技术相结合,实现了富集-原子吸收法联用测定矿样中的锰,该方法检出限(3σ)为0.018μg/L,线性范围0.01—0.5μg/L,相对标准偏差RSD为3.59%。该法应用于标准样品的测定其结果与标准样值相符。应用于实际矿样的测定,加标回收率在96.7%-104.3%之间,结果满意。
A rapid and sensitive method for concentration and separation of trace manganese based on ion exchange process has been developed. The detection limit of the method is 0. 018μg/L. The recoveries are in the range of 96.7% to 104.3% and The relative standard deviations(RSD) are 3.59%. The method has been successfully applied for the determination of manganese in certified reference material GBW07268 and other sample.
出处
《东北电力大学学报》
2006年第1期48-50,共3页
Journal of Northeast Electric Power University
关键词
离子交换分离富集
原子吸收光谱法
测定
锰
Ion exchange process
Separation and Pro -concentration
AAS
Manganese