摘要
目的:建立六神丸(蟾酥,雄黄,麝香等)中总砷的测定方法,研究六神丸在人工肠液中可溶性砷含量。方法:采用原子荧光光谱法。结果:六神丸在人工肠液中的可溶性砷仅占总砷含量的10.5%左右,在短时间内达到溶出平衡,而且人工肠液中的胰蛋白酶对砷的溶出有促进作用。结论:原子荧光光谱法测定六神丸中总砷的方法操作简便,定量准确。
AIM： To establish a method of determining the content of total arsenic in Liushen Pill（Bufonis venenum,Realgar,moschus）,and to research the content of soluble arsenic of Liushen Pill in artificial intestinal juice. METHODS： Atomic fluorescence spectrometry（AFS） was used in this paper. RESULTS： The content of soluble arsenic of Liushen Pill in artifical intestinal juice was only 10. 5% of the total arsenic,and could reach a dissolvable balance in a short time. And the trypsinase in artificial intestinal juice had a promoting effect on the dissolution of arsenic. CONCLUSION： This determination method of total arsenic of Liushen Pill by AFS is simple and has a good quantification result.
出处
《中成药》
CAS
CSCD
北大核心
2010年第8期1352-1354,共3页
Chinese Traditional Patent Medicine
关键词
原子荧光光谱法
六神丸
总砷
可溶性砷
人工肠液
atomic fluorescence spectrometry（AFS）
Liushen Pills
total arsenic
soluble arsenic
artificial intestinal juice
