摘要
采用溶胶凝胶燃烧法在800℃合成了掺杂Ce3+和Tb3+的MgO-Al2O3体系发光材料,比传统高温固相扩散法的合成温度降低了700~800℃.研究了MgO-Al2O3基质当中单掺杂Tb3+及共掺杂Ce3+、Tb3+的发光材料荧光光谱行为,以及恒定温度下时间与浓度对发光材料荧光光谱行为的影响,并对其红外光谱和反应原理进行了探讨.
The luminescence materials of MgO-Al2O3 : Tb^3 + , Ce^3 + have been synthesized by Sol-gel combustion method at 800℃, that is lower 700--800℃; than that of the high temperature solid method. Behavior of fluorescence spectrum doped different concentration of Tb^3+ and Tb^3+/Ce^3+ in MgO-Al2O3 and effect of heated different time at same temperature have been discussed. IR spectrum and reaction principle are also exploringly explained.
出处
《延边大学学报(自然科学版)》
CAS
2005年第4期272-275,共4页
Journal of Yanbian University(Natural Science Edition)
基金
国家自然科学基金资助项目(20261006)
吉林省科技厅基金资助项目(20040506-2)
关键词
溶胶-凝胶-燃烧法
稀土
荧光光谱
反应原理
Sol-gel combustion method
rare earth
fluorescence spectrum
reaction principle