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水热法合成BaNd_xFe_(12-x)O_(19)铁氧体的研究 被引量:9

Synthesis of BaNd_xFe_(12-x)O_(19) Ferrite by Hydrothermal Process
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摘要 本文利用水热法合成了六角形磁铅石结构的BaNdxFe(12-x)O(19)铁氧体,用X射线衍射仪、透射电子显微镜和振动样品磁强计等仪器对粉末的结构、形貌和磁学性能进行了研究,并讨论了Nd(3+)对钡铁氧体磁学性能的影响。结果表明,Nd(3+)可以明显提高BaFe(12)O(19)粉末的矫顽力。 The hexagonal BaNd_xFe_(12-x)O_(19) ferrites with M-type strusture were synthesized by hydrothermal method. The preparation method, process, and the effects of pH value and temperature were examined in details. Pure Nd-hexaferrites were produced at lower temperature. X-Ray diffractometry, magnetic analysis and transmission electron microscope obervations were used for characterizing the synthesized materials. The results shown that rare earth ion Nd ̄(3+) can improve the magnetic properties of BaFe_(12)O_(19). The coercive force of BaNd_xFe_(12-x)O_(19) is approximately 50% higher than that of BaFe_(12)O_(19). The mechanism of Nd ̄(3+) in BaFe_(12-x)O_(19) was discussed.
机构地区 哈尔滨工程大学
出处 《稀土》 EI CAS CSCD 1996年第2期14-17,共4页 Chinese Rare Earths
基金 黑龙江省自然科学基金吉林大学无机水热合成实验室
关键词 水热法 稀土 铁氧体 Ferrite Rare earth Hydrothermal method.
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参考文献3

  • 1Lin C H,IEEE Trans Magn,1990年,26卷,1期,15页
  • 2Yang Zheng,IEEE Trans Magn,1987年,23卷,3131页
  • 3张世远,磁性材料基础,1982年

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