摘要
平台石墨炉原子吸收法直接测定镍基合金中铅和锑谢文兵，姚金玉，胡庆兰（中国科学院长春应用化学研究所长春１３００２２）关键词石墨炉原子吸收，镍合金，铅，锑，基体改进剂石墨炉原子吸收法是测定痕量元素最有效的方法之一。但是铅和锑都是易挥发元素，为了增强灰化过...
The ashing temperature could be increased and some interferences from hy-drochloric acid,molybdenum and boron could be eliminated in title method by using Pd andNias a matrix modifier.The method can be used directly for lead and antimony analysis inhigh temperature nickel-alloy without preseparation of the matrix. The characteristic mass is28pg and 26pg, the detection limit is 0.13μg/g and 0.23μg/g,the recovery is 94%～103%and 95%～110%,the relative standard deviation is 6.4%～7.6%and 4.7%～7.5%for leadand antimony,respectively。
出处
《应用化学》
CAS
CSCD
北大核心
1995年第4期108-110,共3页
Chinese Journal of Applied Chemistry
关键词
原子吸收
镍合金
铅
锑
graphite furnace atomic absorption,nickel alloy,lead,antimony,matrix modifier
