摘要
目的建立GC/ECD、GC/MS分析焚烧尸体肝组织中安定、舒乐安定的方法。方法采用酸性丙酮-水浸提、液-液分配净化的方法,以HP6890GC/ECD、OV-1701石英毛细管柱和岛津QP5050ADB-5MS石英毛细柱分析方法。结果该提取方法的回收率安定81.2%、舒乐安定75.8%,焚烧尸体肝组织中的含量:安定0.060μg/g,舒乐安定0.330μg/g。结论该方法操作简单,准确可靠,适用于中毒案件鉴定。
The samples of the liver tissue of a burned corpse from a poison case were extracted by acidic aceton-water and analysed by GC/ECD and GC/MS.Diazepam and estazolam were found in the burned corpse.Also the contents of the two medicne were determined.
出处
《刑事技术》
2003年第5期22-23,共2页
Forensic Science and Technology
