摘要
为了制得高纯度的三十烷醇-1,采用萃取、皂化、分离、结晶和保温双溶剂交替结晶纯化方法,所得的三十烷醇-1,经气相色谱分析纯度可达99.99％。
High-purty 1-triacontanol was obtained by extraction, saponification, separation. crystallization and recrystallization under constart temparature using two kinds of solvents in turn. The putty of 1-triacontanol identified by gas-phase chromatograghic analysis has been up to 99.99％.
关键词
三十烷醇
萃取
蜂蜡
皂化
1-tracontanol
extraction
derivative
beeswax
saponification
hydrolysis
