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2-乙酰氨基3,4,6-三乙酰葡萄糖的合成 被引量：1

Synthesis of 2-acetylamino-3,4,6-triacetate-D-glucopyranose
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摘要 2acetylamino3,4,6triacetate Dglucopyranose is an important imtermediate in the synthesis of Lipid A analogs.It was synthesized by the regioselective 1Odeacylation of fully acylated sugars.In this paper, the fully acylated aminoglucose was synthesized by a new method.In comparison with the old procedure,the reaction time was shorten ed,yet the yield was still higher. 2acetylamino3,4,6triacetate Dglucopyranose is an important imtermediate in the synthesis of Lipid A analogs.It was synthesized by the regioselective 1Odeacylation of fully acylated sugars.In this paper, the fully acylated aminoglucose was synthesized by a new method.In comparison with the old procedure,the reaction time was shorten ed,yet the yield was still higher.
作者 季卫刚 赵先英 王祥智 覃军 刘毅敏
机构地区 第三军医大学化学教研室
出处 《化学研究与应用》 CAS CSCD 北大核心 2003年第1期97-98,共2页 Chemical Research and Application
关键词 2-氨基葡萄糖五乙酸酯 乙酰化 2-乙酰氨基-3 4 6-三乙酰葡萄糖 2-acetylamino-3,4,6-triacetate -D-glucopyranose acylation 2-acetylamino-2-deoxy-1,3,4,6-tetraacetate-D-glucopyranose
分类号 O629.11 [理学—有机化学]
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参考文献1

  • 1汪猷 戴行义.化学学报,1958,24:368-374.

同被引文献8

  • 1陈仙海,张惟杰.多酶体系催化从1－磷酸葡萄糖和N－乙酰基葡萄糖胺合成N－乙酰基乳糖胺[J].浙江大学学报（自然科学版）,1995,29(5):635-637. 被引量：1
  • 2彭云丽,李静,耿美玉.sLe^(a/x)与肿瘤血源性转移研究进展[J].中国生物工程杂志,2007,27(6):92-95. 被引量：3
  • 3Danishesfsky S J,Behar V, Randolph J T,et al. Application of the Glycal Assembly Method to the Concise Synthesis of Neoglycoconjugates of Ley and Leb Blood Group Determinants and of H-Type I and H-Type II O-0ligosaccharides [J]. Am Chem Soc, 1995,117 : 5701-5711.
  • 4Spassova M K, Bornmann W G, Ragupathi G,et al. Synthesis of Selected LeY and K H-1 Analogues:a Medicinal Chemistry Approach to Vaccine Optimization[J]. Org Chem ,2005,70,3383-3395.
  • 5Sandoval M, Ferreras E, Perez-Sanchez M, et al. Screening of Strains and Recombinant Enzymes from Thermus Thermophilus Fortheir use in Disaccharide Synthesis [J]. Mol Catal B :Enzym,2012,74:162-169.
  • 6Wrodnigg T M,Stutz A E. The Heyns Rearrangement Revisited:an Exceptionally Simple Two-step Chemical Synthesis of D-lactosamine from Lactulose[J]. Angew Chem Int Ed Engl , 1999,38(6) :827-828.
  • 7Yasuhito Nagai,Naoyuki lto,Israt Sultana,et al. Regioandchemoselective Manipulation Under Mild Conditions on Glucosamine Derivatives for Oligosaccharide Synthesis and Its Application Toward N -acetyl- d -lactosamine and Lewis X Trisaccharide[J]. Tetrahedron, 2008,64 : 9599-9606.
  • 8Manuel Sandoval, Concepion Civera, Jose Berenguer, et al. Hernaiz. Optimised N-acetyl-D-lactosamine Synthesis Using Thermus Thermophilus b-galactosidase in bio-solvents[J]. Tetrahedron, 2013,69.1148-1152.

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化学研究与应用
2003年 第1期

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