摘要
以对 -硝基酚与氯化苄、2 ,4-二硝基酚与乙基溴在二甲基亚砜溶剂中进行缩合反应 ,合成了对 -硝基苯基苄基醚和 2 ,4-二硝基苯基乙基醚。考察了不同反应条件下的反应结果 ,结果表明 ,在最佳条件下对 -硝基苯基苄基醚和 2 ,4-二硝基苯基乙基醚的收率分别为 84.9%和 72 .3 %。
The 4-Nitrophenyl Benzyl Ether and 2,4-Dinitrophenyl Ethyl Ether have been synthesized by the reaction of 4-Nitrophenol with benzylchloride and 2,4-Dinitrophenol with ethylbromide in solvent DMSO. Various factors that affect the condensation are discussed.The results show that the yield of 4-Nitrophenyl Benzyl Ether is 84.9 %, and the yield of 2,4-Dinitrophenyl Ethyl Ether is 72.3 %.
出处
《佛山科学技术学院学报（自然科学版）》
CAS
2002年第4期57-59,共3页
Journal of Foshan University(Natural Science Edition)
