摘要
The synthesis of isoamyl hexanoate with isoamyl alcohol and hexanic acid as reactants and sodium bisulfate as catalyst had been studied.The factors affecting reaction were investigated.The results showed that the appropriate conditions should be:Weight of catalyst was 0.5g(weight of hexanic acid if 0.2mol);molar ratio of isoamyl alcohol to hexanic acid was 1.2∶1;reaction time was 1.0h;the taking water reagent(Toulene) was 10ml.The yield of isoamyl hexanoate was as high as 96.8%.
The synthesis of isoamyl hexanoate with isoamyl alcohol and hexanic acid as reactants and sodium bisulfate as catalyst had been studied.The factors affecting reaction were investigated.The results showed that the appropriate conditions should be:Weight of catalyst was 0.5g(weight of hexanic acid if 0.2mol);molar ratio of isoamyl alcohol to hexanic acid was 1.2∶1;reaction time was 1.0h;the taking water reagent(Toulene) was 10ml.The yield of isoamyl hexanoate was as high as 96.8%.
出处
《化学研究与应用》
CAS
CSCD
北大核心
2002年第1期114-115,共2页
Chemical Research and Application
