摘要
为获得天然高分子化合物黑芝麻中黑色素的分子结构信息 ,对其进行碱熔降解 ,然后对降解产物进行硅烷化衍生 ,再利用气相色谱 /质谱联用分析 ,结果发现产物中含有儿茶酚、对苯二酚和儿茶酸 ,从而证明黑芝麻中的黑色素具有儿茶酚型黑色素的结构特征。
Black sesame melanin, a kind of biopolymer was degraded by alkali fusion to study structure characterization The degraded products were derivatized with bis (trimethylsilyl)trifloroacetamide in a sealed tube at 125 ℃ for 30 min The silylanization derivatives of degradation products were analyzed by GC/MS Catechol, 1,4 dihydroxy benzene and catechuic acid were detected This method can be used to characterize the structure type of black sesame melanin
出处
《色谱》
CAS
CSCD
北大核心
2001年第3期268-269,共2页
Chinese Journal of Chromatography
基金
山东省教委资助
