摘要
采用毛细管气相色谱及色谱 -质谱法分析了两种不同催化剂催化合成笼状烃金刚烷反应体系的各主要组分。给出了测试条件和标准曲线。对于AlCl3 催化反应体系各组分回收率在98 %～101 %之间 ,RSD<5.0 %。对于沸石催化反应体系 ,各组分回收率在96 %～103 %之间 ,RSD<7.0 %。该法定量分析快速、简便。
Products of adamantane synthesis for two catalytic systems were determinated by capillary gas chromatography and gas chromatography-mass spectrometry. The detection conditions and standard curves were given. The recoveries of 96%～103% and the RSDs of less than 7.0% were obtained for zeolites catalytic system components, while the recoveries of 98%～101% and the RSDs of less than 5.0% were achieved for AlCl3 catalytic system components. The method is rapid, simple and accurate.
出处
《分析测试学报》
CAS
CSCD
北大核心
2001年第4期56-58,共3页
Journal of Instrumental Analysis
