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HS-SPME-GC-MS联用分析沙苑子中挥发性成分 被引量:3

Analysis of Volatile Constituents of Astragali Complanati Semen by HS-SPME Combined with GC-MS
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摘要 目的:分析沙苑子中挥发性成分的化学组成。方法:采用顶空固相微萃取法(HS-SPME)萃取沙苑子中挥发性成分,并用气相色谱-质谱(GC-MS)联用技术对沙苑子的挥发性成分进行分析。结果:从沙苑子中共分离出51个色谱峰,鉴定出其中25种化合物,占总量的78.85%。其中主要成分为L-乙酸龙脑酯(14.10%)、樟脑(5.98%)、右旋龙脑(4.27%)等。结论:首次采用HS-SPME-GC-MS联用技术分析沙苑子挥发性成分,为沙苑子的进一步开发利用提供了科学依据。 Objective: To analyze the compositions of volatile constituents in Astragali Complanati Semen. Methods: The volatile constituents were extracted with headspace solid phase micro extraction( HS-SPME),and identified by GC-MS. Results: 51 compounds were separated from Astragali Complanati Semen and 25 of them were identified,which made up 78. 85% of the total amount. The main components obtained from Astragali Complanati Semen were L-Bornyl acetate( 14. 1%),Camphor( 5. 98%) and L(-)-Borneol( 4. 27%). Conclusion: The compounds in Astragali Complanati Semen are firstly confirmed,which provides scientific evidence for the development of Astragali Complanati Semen.
出处 《中药材》 CAS CSCD 北大核心 2013年第12期1966-1968,共3页 Journal of Chinese Medicinal Materials
关键词 沙苑子 顶空-固相微萃取 气相色谱-质谱联用 挥发性成分 Astragali Complanati Semen HS-SPME GC-MS Volatile components
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