摘要
探讨了腐霉利的气相色谱分析方法 ,采用氢焰离子化检测器 ,5% OV- 1 0 1 Chromosorb G.AWDMCS填充的 1 .0 m× 3mm i.d玻璃柱 ,柱温 2 50℃ ,检测室和汽化室温度 2 70℃ ,以邻苯二甲酸二辛酯为内标物。实验结果为 :回收率在 1 0 0 .0 %～ 1 0 3.6% ,变异系数≤ 0 .1 1 %。
Procymidone was determined by gas chromatography with hydrogen flame ionization detector and a 1.0 m×3 mm i.d.glass column packed with 5% OV 101 chromosorb G.AW DMCS. The column, injector and detector temperature was 250℃,270℃ and 270℃ respectively. Dioctyl phthalate was used as internal standard. The recovery was between 100%~103.6%, and the coefficients of variation was less than 0.11%.
出处
《广西化工》
2000年第3期39-40,共2页
Guangxi Chemical Industry
