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火焰原子吸收光谱法对妇科用药中微量元素的测定

Determination of Trace Elements in Herbal Drugs for Gynaecology by Flame Atomic Absorption Spectrometry
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摘要 目的:为4种治疗妇科疾病常用中草药(当归、艾叶、川芎、益母草)的进一步研究提供参考数据。方法:采用HNO3和HClO4(4+1)消解样品,用火焰原子光谱吸收法测定4种治疗妇科疾病常用中草药(当归、艾叶、川芎、益母草)中Fe、Zn、Mn微量元素的含量。结果:4种治疗妇科疾病中草药中都富含微量元素铁,锌和锰含量较少,其顺序为Fe〉Zn〉Mn。结论:方法回收率在96.0%~106.4%之间,RSD在0.59%~1.8%之间,准确可靠,为4种中草药的进一步研究提供参考数据。 Objective: The present study provides scientific evidence for further study of four kinds of Chinese Traditional and Herbal Drugs for Gynaecology. Methods: The flame atomic absorption spectrometry (FAAS) was applied to determine the trace elements including Fe, Zn and Mn on the basis of digesting the sample by a concentrated nitric acid and perchloric acid (4:1 V/V) for four kinds of Chinese Traditional and Herbal Drugs for Gynaecology. Results: The results obtained show that the content of Fe, Zn and Mn are abundant, Sequence of Total amount is Fe〉Zn 〉 Mn. Conclusion:The recoveries were between 96.0 % -106.4 %, Root mean square deviations were between 0.59 % -- 1.8 % , which indicate the method is reliable.
出处 《微量元素与健康研究》 CAS 2013年第6期29-30,共2页 Studies of Trace Elements and Health
关键词 火焰原子吸收法 妇科中药 微量元素 Flame atomic absorption spectrometric method trace elements
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