摘要
用固体超强酸 Ti O2 / SO- 24 -沸石分子筛催化合成尼泊金酯 ,对催化剂的制备条件和尼泊金丙酯的合成条件进行了研究。在最佳反应条件下 ,尼泊金丙酯的产率为93.5 %。实验还表明 ,此催化剂与单组分固体超强酸 Ti O2 / SO- 24 相比 ,具有成本较低的优点 ,且具有重复使用性 ,是合成尼泊金酯的良好催化剂 ,具有较好的应用前景。
The synthesis of Nipagin esters with zeolite supported TiO 2/SO -2 4 solid super acids as catalysts was studied, including the preparation of catalyst and esterification conditions. Under optimum synthetic condition, the yield of propyl ester was 93.5%. Compared with blank TiO 2/SO -2 4 solid super acid, this complex catalystis cheaper and can be used repeatedly. It showed that this complex catalyst was an excellent one for the synthesis of Nipagin esters.
出处
《化学世界》
CAS
CSCD
2000年第12期641-644,共4页
Chemical World
基金
江西省自然科学基金!资助项目 (96 2 12 7)
