摘要
文章在溶液中温和的条件下合成了四硝基酞菁钴和四氨基酞菁钴配合物,该方法具有反应温度低、毒性小、产率高等特点,两种产物产率分别为60.0%和89.6%。并探索出柱层析法分离提纯四硝基酞菁钴的方法。通过紫外可见分光光度计和核磁共振仪对产物进行了表征。
In the paper, we synthesized the phthalocyanine complexes of tetranitro-phthalocyanine cobalt and tetroamino-phthaloeyanine cobalt under mild conditions. This synthesis method had characteristics of low reaction temperature, low toxicity and high yield and so on. The yield of the two products were 60.0 % and 89.6 %. And we explored a way of separation and purification of tetronitro-phthalocyanine cobalt by column chromatography. What＇s more, the products were characterized by UV-Vis spectrophotometer and NMR spectrometer.
出处
《广东化工》
CAS
2013年第17期13-14,共2页
Guangdong Chemical Industry
关键词
温和条件
酞菁配合物
分离提纯
mild conditions
phthalocyanine complexes
purification
