摘要
以金属氯化物和吡啶共同作为催化剂 ,在惰性有机溶剂中 ,用氯化铵和五氯化磷反应合成了六氯环三磷腈 ,该法反应时间短 ,产率可高达 87%。
Hexachlorocyclotriphosphazene was prepared by reacting ammonium chloride and phosphorus pentachloride in an inert organic solvent at the presence of metal chloride and pyridine. The yield of hexachlorocyclotriphosphazene can reach 87% under the suitable condition, while reducing the reaction time.
出处
《氯碱工业》
CAS
2000年第8期27-28,共2页
Chlor-Alkali Industry
关键词
六氯环三磷腈
氯化铵
五氯化磷
合成
催化
hexachlorocyclotriphosphazene
ammonium chloride
phosphorus pentachloride
synthesis