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气相色谱法测定有机磷杀虫剂噁唑磷 被引量:1

Determination of the Mildew Preventive,Dimethyl Fumarate by Gas Chromatography
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摘要 采用气相色谱法在 5%OV - 1 0 1 /ChromosorbW -AWDMCS色谱柱上分离和测定有机磷杀虫剂唑磷含量。该方法操作简便、快速、准确可靠。对同一试样的 5次平行独立测定的标准偏差为 0 .1 5,变异系数为 0 .55%;并且 ,标准加入法回收率达 98.2 0 %~ 1 0 2 .4%。 In this paper,the separation and determination of insecticide isoxathion had been studied by gas chromatography on the 5%OV-101/Chromosorb W-AW DMCS chromatographic column.The method possesses simple,fast,accurate and precious.Ten-time analysis of a same sample gave a mean value of 27.82% with the method standard deviation 0.51,and a coefficient of variation of 0.52%.The recovery of the method for dimethyl fumarate was 98.20%~102.4%.
作者 施介华
出处 《农药》 CAS 北大核心 2000年第7期16-17,共2页 Agrochemicals
关键词 杀虫剂 恶唑磷 气相色谱法 有机磷杀虫剂 insecticide,isoxathio,gas chromatography,determination.
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参考文献3

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共引文献4

同被引文献8

  • 1Kazuo Sato, Soji Sugai, Kazuo Tomita. Synthesis of 3 - Hydroxyisoxazoles from β- Ketoesters and Hydroxylamine. Agric.Biol. Chem, 1986, 50(7): 1831-1837.
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  • 3江藤永凇.有机磷农药的有机化学与生物化学.北京:化学工业出版社,1981.
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  • 7杨忠愚,蔡志彬,孙楠,胡惟孝.3-羟基-5-苯基异噁唑的合成研究[J].浙江工业大学学报,1997,25(4):320-325. 被引量:1
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