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固-液相转移催化法合成N-芳基N′-(α-萘甲酰基)硫脲和芳撑-二(α-萘甲酰基)硫脲衍生物 被引量：1

Phase transfer catalyzed synthesis of N-aryl-N′-(α- naphthoyl) thiourea and arene bis(α- naphthoyl)thiourea derivatives
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摘要 在固 液相转移催化下 ,以PEG 4 0 0为催化剂 ,通过α 萘甲酰氯与硫氰酸铵以及芳胺和芳二胺反应 ,合成了一系列N 芳基 N′ (α 萘甲酰基 )硫脲和芳撑 二 (α 萘甲酰基 ) By reaction of aromatic amines or arene diamines with α naphthoyl chloride and ammonium thiocyanate under the condition of solid liquid phase transfer catalysis using PEG 400 as the catalyst a series of N aryl N′ ( α naphthoyl)thiourea or arene bis( α naphthoyl)thiourea derivatives are synthesized.
作者 魏太保 张有明
机构地区 西北师范大学化学化工学院
出处 《西北师范大学学报（自然科学版）》 CAS 2000年第3期39-42,共4页 Journal of Northwest Normal University(Natural Science)
基金 国家自然科学基金资助项目!(29971026) 甘肃省中青年自然科学基金资助项目!(YS991A250 0 5)
关键词 芳基 萘甲酰基 硫脲 芳撑 萘甲酰基 相转移催化 N-aryl-N' (α-naphthoyl)thioureas arene bis(α- naphthoyl)thioureas synthesis phase transfer catalysis
分类号 O623.543 [理学—有机化学]
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参考文献6

  • 1SchroederDC.Thioureas[J].ChemRev,1955,55:185—228．
  • 2ZhangYou-ming,WeiTai-bao.PhasetransfercatalyzedsynthesisofN-aryl-N′-(2-chlorobenzoyl)thioureaderivatives[J].SynthCommun,1997,27(5):751—756．
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同被引文献10

  • 1Mohanazadeh F,Aghvami M.2-Hydroxy-N,N,N-tributylethanaminium thiocyanate as solvent and reagent for the preparation of alkyl thiocyanates[J].Tetrahed Lett,2007,48(40):7240-7242.
  • 2Bellomo A,Gonzalez D.Diasterodivergent synthesis of optically pure vinyl episulfides and β-hydroxy thiocyanates from a bacterial metabolite[J].Tetrahed Lett,2007,48(17):3047-3051.
  • 3Ju Y,Kumar D,Varma R S.Revisiting nucleophilic substitution reactions:microwave-assisted synthesis of azides,thiocyanates,and sulfones in an aqueous medium[J].J Org Chem,2006,71 (17):6697-6700.
  • 4Burski J,Kieszkowski J,Michalski J.Synthesis of isothiocyanatophosphoranes and iso-thiocyanato phosphonium salts via oxidative addition of thiocyanogen and ligand substitution:novel reagents for converting hydroxy groups into thiocyanate and isothiocyanate functions under mild conditions[J].Tetrahedron,1983,39(24):4175-4181.
  • 5Du Y F,Cao Y Q,Dai Z.A study on the heterogeneous reaction of trialkylsilyl chlorides with inorganic salts and monocarboxylates catalyzed by PEG400[J].Journal of Chemical Research,Synopses,2004,3:223-225.
  • 6Karade N N,Tiwari G B,Shirodkar S G.Efficient and mild oxidative nuclear thiocyanation of activated aromatic compounds using ammonium thiocyanat and diacetoxyiodobenzene[J].Synthetic Communications,2005,35(9):1197-1201.
  • 7Khazaei A,Alizadeh A,Vaghei R G.Preparation of arylthiocyanates using N,N-'-dibromo-N,N-'-bis(2,5-dimethylbenzenesulphonyl) ethylenediamine and N,N-dibromo-2,5-dimethyl benzene sulphonamide in the presence of KSCN as a novel thiocyanating reagent[J].Molecules,2001,6(3):253-257.
  • 8王园园,宋华,柳艳修.微波促进有机合成化学的应用进展[J].天津化工,2008,22(5):11-14. 被引量：12
  • 9俞善信,徐满才,李善吉.聚氯乙烯多乙烯多胺树脂催化合成硫氰酸苄酯[J].离子交换与吸附,1998,14(2):129-132. 被引量：3
  • 10臧洪俊,李正名,王宝雷.固态有机合成反应进展[J].有机化学,2003,23(10):1058-1063. 被引量：30

引证文献1

西北师范大学学报（自然科学版）
2000年 第3期

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