摘要
目的提高枣仁安神颗粒的质量标准。方法采用薄层色谱法对枣仁安神颗粒进行鉴别;采用高效液相法测定其有效成分含量。结果薄层色谱法可鉴别出与酸枣仁、丹参、五味子中的特征斑点;高效液相色谱法测定丹参中的丹参酮ⅡA,在测定范围内线性良好,回收率在97%~101%之间。结论所建立的质量标准简便可行、重复性好,可作为枣仁安神颗粒的质量监控。
OBJECTIVE To improve a quality standard for Zaoren Anshen granules.METHODS Zaoren Anshen granules was identified by TLC;the effective components in Zaoren Anshen granules were determined by HPLC.RESULTS The characteristics spots in Spine Date Seed,Salvia and Schisandra Chinensis were identified by TLC;the tanshinoneⅡA of Salvia in Zaoren Anshen Granules were well-separated with good linearity within its concentration range.And the recoveries were within 97%～101%.CONCLUSION The quantitative method for determinating the ingredients of Zaoren Anshen Granules is simple,feasible and repeatable,and is beneficial for quality control of Zaoren Anshen Granules.
出处
《海峡药学》
2012年第9期58-60,共3页
Strait Pharmaceutical Journal
