摘要
以钛酸四丁酯为主要原料,氯化锌溶液为掺杂剂,采用超声分散法制备了含锌的二氧化钛光催化剂.并采用X射线衍射(XRD),透射电镜(TEM)对产品进行了表征.同时研究了不同影响因素对苯酚去除率的影响.结果表明,焙烧温度为500℃,锌掺杂量r(Zn∶Ti)=0.01,催化剂的最佳投加量为2 g/L光催化性最好.
Zn doped titanium dioxide photocatalyst were prepared via ultrasonic dispersion method. Tetrabutyl titanate was main raw material, zinc chloride solution was a doping agent. The structure and morphology of the asprepared samples were characterized by X - ray diffraction (XRD) and transmission electron microscopy (TEM). At the same time, the different influence factors on the removal efficiency of phenol were studied. When calcinations temperature was 500 ℃, the amount of zinc doped r ( Zn: Ti ) was 0.01, catalyst dosage was 2 g/ L , the photocatalysis was optimum.
出处
《哈尔滨商业大学学报(自然科学版)》
CAS
2012年第2期140-142,共3页
Journal of Harbin University of Commerce:Natural Sciences Edition
基金
黑龙江省自然科学基金资助项目(B200902)
关键词
二氧化钛
锌掺杂
超声分散法
光催化剂
titanium dioxide
zinc doped
ultrasonic dispersion method
photocatalyst