期刊文献+

低场核磁共振技术检测煎炸油品质 被引量:53

Application of Low-Field Nuclear Magnetic Resonance(LF-NMR) to Analyze Frying Oil Quality
在线阅读 下载PDF
导出
摘要 应用低场核磁共振技术对无对象煎炸大豆油油样进行检测,通过对多组分T2弛豫图谱以及峰面积比例S21和单组份弛豫时间T2w分析,煎炸4h后图谱中10ms左右出现明显特征小峰,且S21和T2w与煎炸时间、酸价、黏度、吸光度和极性组分含量呈现良好的规律性,相关系数在0.941~0.997之间,说明可以利用低场核磁共振检测的S21和T2W有效反映煎炸油的品质变化。但与过氧化值之间无明显规律性。结果可为后期煎炸油的低场核磁共振技术快速检测提供基础。 Low-field nuclear magnetic resonance(LF-NMR) was used to analyze soybean oil without objects in it during frying.Multi-component T2 relaxation spectra,peak area ratio S21 and single component relaxation time T2w were determined.An obvious characteristic peak appeared at 10 ms in the multi-component T2 relaxation spectrum after 4 h of frying.S21 and T2w were correlated with frying time,acid value,viscosity,absorbance and polar component content with a correlation coefficient between 0.941 and 0.997.Thus,S21 and T2w could effectively reflect the quality of frying oil.However,they had no obvious correlation with peroxide value.These results will be very helpful for the application of LF-NMR to rapidly detect frying oil quality.
出处 《食品科学》 EI CAS CSCD 北大核心 2012年第6期171-175,共5页 Food Science
基金 上海市教委科研创新项目(11YZ109)
关键词 低场核磁共振 煎炸油 快速检测 T2弛豫图谱 low-field nuclear magnetic resonance(LF-NMR) frying oil rapid detection T2 relaxation spectrum
  • 相关文献

参考文献18

二级参考文献55

  • 1黄兴,姚庭香,王吉良,徐风.煎炸油质变检验方法探讨[J].食品科学,1995,16(8):50-53. 被引量:17
  • 2朱向菊,裘爱泳,金青哲.以猪油分提固脂为原料的起酥油的研制[J].中国油脂,2005,30(8):11-14. 被引量:14
  • 3黄道平,彭进,谢燕湘,孟霞.潲水油鉴别检测方法研究[J].中国卫生检验杂志,2006,16(2):151-153. 被引量:44
  • 4张蕊,祖丽亚,樊铁,赵科鹏.测定胆固醇含量鉴别地沟油的研究[J].中国油脂,2006,31(5):65-67. 被引量:106
  • 5Fragaki G, Spyros A, Siragakis G, et al. Detection of extra virgin olive oil aduheration with lampante olive oil and refined olive oil using nuclear magnetic resonance spectrosco - PY and multivariate statistical analysis [ J ]. J Amc Food Chem,2005,53(8) :2 810 -2 816.
  • 6Vigli G, Phihppidis A, Spyros A, et al. Classification of edible oils by employing 31p and 1H NMR spectroscopy in combination with multivariate statistical analysis. A proposal for the detection of seed oil adulteration in virgin olive oils[J]. J Agica Food Chem,2003,51 (19):5 715 -5 722.
  • 7Blumenthal M M.A new look at the chemistry and physics of deep fat frying[J].Food Technology,1991,45(2):68-72.
  • 8Clark W L,Serbia G W.Safety aspects of frying fats and oils[J].Food Technology,1991,45(2):84-89.
  • 9White P J.Methods for measuring changes in deep-fat frying oils[J].Food Technology,1991,45(2):75-80.
  • 10Tyagi V K,Vasishtha A K.Changes in the characteristics and composition of oils during deep-fat frying[J].J.Am.Oil Chem.Soc.,1996,73(4):499-506.

共引文献186

同被引文献729

引证文献53

二级引证文献397

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部