摘要
以三乙胺为模板剂,用水热晶化法,首次在非酸性介质中合成了SAPO-5、SAPO-34型分子筛.通过X-射线粒未衍射、电子探针微区分析、电子能谱及红外光谱进行了结构研究,确认合成样品为SAPO-5和SAPO—34型分子筛,并对它们的化学组成、热稳定性、表面酸性及吸附性能进行了研究。
The molecular sieves SAPO-5 and SAPO-34 have been synthesized hydrothermally in the presence of triethylamine templates in non-acid medium. The determination X-ray diffraction, electron scanning microscope, X-ray photoelectron spectroscopy, infrared spectrum showed the difference of the two kinds of silicoaluminophosphate molecular sieves. Some properties, including thermal stability, surface acidity and adsorption property, have been studied.
出处
《无机化学学报》
SCIE
CAS
CSCD
北大核心
1990年第2期176-180,共5页
Chinese Journal of Inorganic Chemistry
关键词
分子筛
磷酸硅铝
合成
非酸性介质
molecular sieve silicoaluminophosphate triethylamine non-acid medium