摘要
目的：建立洗必灵洗剂的质量控制方法。方法：采用薄层色谱法对洗必灵洗剂中苦参、黄柏、蛇床子三味中药材进行定性鉴别,以高效液相色谱法对其主要药材苦参中的苦参碱进行含量测定。结果：苦参、黄柏、蛇床子的供试品薄层色谱中,在与对照品相同位置上显相同颜色的斑点;苦参碱在14~560μg.mL-1浓度范围内与峰面积积分值呈良好线性关系（r=0.9999）,平均回收率为98.2%,RSD=2.55%（n=6）。结论：本方法简便、准确、灵敏、重现性好,可用于本品的质量控制。
Objective:To establish a xibiling in the quality control lotion.Methods:TLC on xibiling lotion flavescens,Cork,Cnidium shamisen Chinese herbal medicine were identified according to HPLC of its main ingredients were matrine in matrine determination.Results:flavescens,Cork,Cnidium of the testsample by TLC,in the same position with the reference substance were the same color of the spots;matrine concentration in the range of 14~560μg·mL-1 integral value of peak area was a good line sexual relationship(r=0.999 9),the average recovery was 98.2%,RSD=2.55%(n=6).Conclusion:This method is simple,accurate,sensitive,reproducible,and available for quality control.
出处
《亚太传统医药》
2011年第5期14-16,共3页
Asia-Pacific Traditional Medicine
