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用自动划痕仪测定硬质镀层的结合强度 被引量:3

Measuring Adhesive Strength of Hard Coatings with an Automatic Scratch Tester
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摘要 作者利用自制的自动划痕试验仪对通过等离子增强化学气相沉积法(PECVD)制备的TiN和TiC镀层进行了划痕试验,考察了底材硬度、镀层厚度、镀层硬度、加载速率、划痕速度及压头(亦称划针)、与镀层间的摩擦状况等因素对表征镀层结合强度的临界载荷的影响。结果表明,临界载荷随底材硬度及镀层硬度的增加而增大,镀层厚度存在一个最佳值,在此值下的临界载荷最大,当加载速率高于100N/min时,临界载荷基本不再受其影响,临界载荷与划痕速度无关,镀层上覆盖固体润滑剂可使临界载荷增大,而覆盖纯油对临界载荷没有影响。 The scratch test for PECVD TiNand TiC coatings using a self-made automatic scratch tester has been, conducted by the authors. The influences of substrate hardness, coatisng hardne,ss, coating thickness, loading rate, scratch speed and the, friction i state between the indenter ( scratcher) and coatings on critical, load,which cha- racters the adhesive strength of coatings, have been studied. The results show that the critical loads of hard coatings increase:s1w.ith increasing of substrate hardness and coating hardness,but with .an optimum coating thipkn.ess, the maximum critical load exists. Since loading rate is higher tluwi 100 N/min, it has no effect on critical load. The critical load is independent of the scratch speed. A solid lubricant film on hard coating can increase its critical load, but a lubricating oil does not have this effect.
出处 《固体润滑》 CSCD 北大核心 1989年第4期224-229,共6页
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参考文献1

  • 1程淑英,王秀娥,徐锦芬.SS-4干膜摩擦磨损性能的研究[J]固体润滑,1982(04).

同被引文献21

  • 1李松辉,陈大凯.PCVD TiN膜基结合强度初探[J].材料保护,1989(8):28-29. 被引量:3
  • 2贾俊辉.表面膜附着力的压痕法测定[J].机械工程材料,1988,12(6):31-33.
  • 3滕风恩 王煜明 等.X射线结构分析与材料性能表征[M].北京:科学出版社,1997..
  • 4S.J.Bull,in W.Gissler andH.A.Jehn(eds).Advanced Techniques for Surface Engineering[M].Kluwer,Dordrecht,1992,31-68.
  • 5D.S.Richerby.A Review of the Methods of the Measurements of Coating-SubstrateAdhesion[J].Surf.Coat.Technol.1988,36:541-557.
  • 6A.J.Perry,J.Valli,P.A Steinman.A Dhesion Scratch Testing:Around-RobinExperiment[J].Surf.Coat.Technol.1988,36(1-2):559-575.
  • 7A.J.Perry,Adhesion Studies of Ion-Plated TiN On Steel[J].Thin SolidFilms,1981,81(4):357-366.
  • 8A.J.Perry,Scratch Adhesion Testing of Hard Coating[J].Thin SolidFilms,1983,107:167-180.
  • 9P.Hedenqvist,S.Hogmark,Experience from Scratch Testing of Tribological PVDCoating[J].Tribology Interntional,1997,30(7):507-516.
  • 10S.J.Bull,D.S.Rickerby,The Use of Scratch Adhesion Testing for the Determination ofInterfacial Adhesion:the Importance of Friction Drag[J].Surf.Coat.Technol,1988,36:503-517.

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