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α-K_7P_2W_(17)FeO_(61)纳米纤维的制备与表征

Synthesizing and Characterizing Nanofibrous of α-K_7P_2W_(17)FeO_(61)
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摘要 运用高压静电纺丝和程序焙烧方法,制备α-K_7P_2W_(17)FeO_(61)纳米纤维丝。通过红外光谱(FTIR),X射线粉末衍射(XRD)进行了表征,结果表明制备的纳米纤维是纯α-K_7P_2W_(17)FeO_(61),扫描电子显微镜照片(SEM)显示焙烧后产物为纳米纤维丝,直径分布图显示其平均直径大约为1 55nm。 The nanofibers of α-K7P2W17FeO61 were obtained through electrospun and calcinations methods. FTIR spectroscopy and XRD showed that nanofibrous polyoxometalates was α-K7P2W17FeO61. Scanning electron microscopy images and diameter distribution curves of the fibrous membranes indicated that the average diameter of α-K7P2W17FeO61 fibers was about 155nm.
作者 隋春红 龚剑 孙永玲
机构地区 吉林医药学院药学院 东北师范大学化学学院
出处 《光谱实验室》 CAS CSCD 北大核心 2010年第6期2427-2430,共4页 Chinese Journal of Spectroscopy Laboratory
基金 教育部归国留学基金项目 吉林省自然科学基金资助项目(20070505)
关键词 静电纺丝 α-K7P2W17FeO61纳米纤维 Electrospinning α-K7P2W17FeO61 Nanofibers
分类号 O657.33 [理学—分析化学] O434.13 [机械工程—光学工程]
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参考文献8

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2010年 第6期

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